Title: Adapted from the Penn State University Radionuclide Safety Training
1Adapted from the Penn State UniversityRadionucli
de Safety Training
- Radiation Safety and
- Protection
- (Created by Russel O. Dunkelberger II, PSU
Environmental and Radiation Protection)
21. Introduction
3Introduction
- University rules and Nuclear Regulatory
Commission (NRC) regulations require that anyone
working with or around ionizing radiation must be
instructed about the possible hazards of
radiation exposure and the procedures to be used
for the safe handling of radioactive materials.
4JC Radiation Safety
- The President is officially responsible to the
NRC for assuring that radioactive material is
used according to the conditions of the NRC
regulations and licenses. - Appoints the Radiation Safety Officer (RSO) to
establish and oversee the policies for the use of
radioactive material - RSO is Dr. Jill Keeney. Assisted by Roy Nagel,
Sciences Safety Director.
5Radiation Safety Program Organization
Juniata College President
Juniata College Provost
Radiation Safety Officer
Science Safety Manager
Faculty and Staff
Research Students
62. Regulations
7NRC Regulations
- Available from EHS
- 10 CFR 19
- Requirements for instruction of personnel
- Posting of Notices and inspections
- 10 CFR 20
- Standards for radiation protection
8Form NRC-3 Notice To Employees
- Posted in or near all radioactive materials use
labs - Lists responsibilities of NRC licensees and
persons working with radioactive material - Provides the address and phone number to contact
the NRC
9Things you should know
- Licensed radioactive material may only be used
by, or under the direct supervision of,
individuals approved by the RSO (almost always
permanent professors). - Licensed radioactive material may not be used in
tracer studies involving direct release of
licensed material to the environment. - Radioactive material may not be administered to
humans or be added to food, beverage, cosmetic,
drug or any other product designed for ingestion
or inhalation by, or application to, humans.
10More things you should know...
- Purchases and/or transfers of radioactive
material are to be made through the RSO. This
includes transfers between authorized users at
the University as well as between the University
and other institutions. - The RSO will not hesitate to impose sanctions on
radionuclide users who do not comply with the
conditions of their authorizations to use
radioactive material.
11Even more things to know...
- Individuals are also subject to civil penalties,
if they willfully violate NRC regulations or
license conditions. - Violations usually result in corrective actions
that affect all persons working with radioactive
material, not just the individuals responsible
for the infractions. - If you have questions about the regulations,
license conditions or procedures, contact the RSO
12Other Regulatory Information
- The University also has to operate under
regulations and licenses issued by the
Pennsylvania Department of Environmental
Resources, Bureau of Radiation Protection. In
general, the state regulations are identical to
those of the NRC. - The Juniata College Radiation Safety Manual
contains rules for working with radioactive
material. A copy of these rules is available at
P\Keeney\P radiation safety\radiation safety
manual and is provided to laboratory supervisors.
1310 CFR 21Notification of Defects
- NRC licensees are required to identify and
evaluate any defects that may potentially be a
substantial radiological safety hazard, and any
situation that leads to failure to comply with
regulations. Such occurrences may need to be
reported to the Nuclear Regulatory Commission. - If you suspect that any facility, activity or
component fails to comply with federal
regulations or creates a substantial radiological
safety hazard, contact the RSO (Dr. Jill Keeney),
or the Safety Director (Roy Nagle) immediately!
143. Properties of Radiation
15Nomenclature
A
- A mass number Z N total number of protons
neutrons - N number of neutrons
- Z atomic number number of protons
- X element
X
Z
16Example
14
C
- A 14 protons and neutrons
- Z 6 protons
- N 8 neutrons
- C Carbon
6
17Radioactive Material, Radiation and Contamination
18Radioactive Material
- Radioactive material is a solid, liquid or gas
compound or mixture in which some of the atoms
present are radioactive atoms
19Radioactivity
- Radioactivity is the natural property of certain
nuclides to spontaneously emit energy, in the
form of ionizing radiation, in an attempt to
become more stable.
20Radiation
- Radiation is the term given to the energy
transmitted by means of particles or waves - It can be ionizing or non-ionizing
21Non-Ionizing Radiation
- Examples
- Microwaves
- Sunlight
- Infrared Waves
- Radio Waves
- Lasers
22Ionizing Radiation
- Ionizing radiation occurs from the addition or
removal of electrons from neutral atoms. Four
main types of ionizing radiation are alpha, beta,
gamma and neutrons.
23Alpha Radiation (?)
- Helium nucleus
- 2 protons and 2 neutrons
- Large, Slow, 2e charge
- High linear energy transfer (LET)
- Low penetrability
- Decay
- Po ? Pb He
210
206
4
2
84
82
24Beta Radiation (?)
- Electron emitted from nucleus
- Small, Fast, -1e charge
- Medium LET
- Medium penetrability
- Decay
- Neutron converted into a proton and an electron
- P? S ?- 1.7 MeV
32
32
15
16
25Gamma (?) and X- Radiation (X)
- Gamma rays and x-rays are photons
- No mass, no charge, travel at speed of light
- Low LET
- High penetrability
- Commonly accompany other radiation
- Penetrability can vary therefore, shielding and
detection requirements vary
26Neutrons (n)
- Neutral particle
- Classified by energy
- Fast neutrons - energy greater than 0.1 MeV
- Thermal neutrons - same kinetic energy as gas
molecules in the same environment - A concern at the nuclear reactor and with soil
moisture probes - Emission of neutrons accompanies the splitting of
Uranium and Plutonium nuclei
27Linear Energy Transfer (LET)
- LET is used to describe the amount of energy
imparted locally by ionizing radiation in a
target. - The higher the value of a particles or waves
LET, the greater the amount of damage that
particle could potentially cause to the target.
28Penetrability
- The ability of radiation to penetrate matter.
- Alpha particles have a low penetrability and can
be shielded by a piece of paper. - Beta particles have a higher penetrability and
are usually shielded with Plexiglas. - Gamma rays have the highest penetrability of the
three, and are shielded with thick concrete or
lead.
29LET and Penetrability
- On the following diagram, each dot represents a
unit of energy deposited. As you will see from
the diagram, alpha particles impart a large
amount of energy in a short distance. Beta
particles impart less energy than alphas, but are
more penetrating. Gamma rays impart little energy
and are the most penetrating. Remember, gamma and
x-rays vary widely in energy. The diagram shows a
high energy gamma ray.
30LET and Penetrability
31Radiation Units
- Exposure
- Charge produced in air from ionization by gamma
and x-rays Unit Roentgens, R - Radiation Absorbed Dose
- Energy deposited by any form of ionizing
radiation in a unit mass of material Unit rad - Dose Equivalent
- Scale for equating relative hazards of various
types of ionization in terms of equivalent risk
Unit rem (1 rem 1,000 mrem)
32Radiation Units
- Activity
- Measure of the amount of radioactivity present
- Units Curie, Ci or Becquerel, Bq
- Becquerel one decay per second (dps)
- Curie dps occurring in the quantity of radon
gas in equilibrium with one gram of radium - 1 Ci 2.22 x 1012 dpm 3.7 x 1010 Bq
- 1 ?Ci 2,220,000 dpm 37,000 Bq
33Half-Life and Decay
- Each radioactive nuclide has its own unique
characteristic pattern of decay, based on - Types (alpha, beta, etc.) and energies of the
emission involved - Rate of decay, or half-life.
- A radionuclides half-life is the amount of time
it takes for one-half of the radioactive atoms
present to disintegrate or decay.
34Decay Calculation
A A0e-?t
- Where
- A Activity at time, t
- A0 Initial activity
- ? ln 2 / half-life
- t Elapsed time
35Example
- If you have 1 mCi of P-32 initially, how much
P-32 would remain after 8 weeks? Assume P-32 has
a half-life of 14 days.
A (1 mCi) e-(Ln 2 / 2 weeks) (8 weeks) Note
that the half-life of 14 days was converted to 2
weeks, so that the units match with the elapsed
time period. A (1 mCi) e-(0.693 / 2 weeks)
(8 weeks) A (1 mCi) e-(.347 / weeks) (8
weeks) A (1 mCi) e-(2.77) A (1 mCi)
(0.0625) A 0.0625 mCi
36Is There an Easier Way?
- There sure is! Draw a chart, as shown below, to
get a quick estimate of activity remaining at
time, t. For 1mCi of P-32,
Elapsed time, t half-lives Activity 0
weeks 0 1 mCi 2 weeks 1 0.5 mCi 4
weeks 2 0.25 mCi 6 weeks 3 0.125 mCi 8
weeks 4 0.0625 mCi
374. Radiation Biology
38Sources of Radiation
- Average person receives 360 mrem per year
- Natural Sources 295 mrem (82)
- Terrestrial 228 mrem
- Human Body 40 mrem
- Cosmic 27 mrem
- Man-made 65 mrem (18)
- Medical 15 mrem
- (chest x-ray 10 mrem)
- Products 10 mrem
- (tobacco, cosmetics, etc.)
- Other 2 mrem
- (occupational, fallout, nuclear power, etc.)
39Biological Effects to Typical Occupational
Exposures
- From NRC Regulatory Guide 8.29
- (available at http//www.nrc.gov/NRC/RG/08/08-029.
pdf) - Assessment of cancer risks associated with
radiation exposure is projected from doses
greater than 10 rem (10,000 mrem) - There is no scientific evidence that conclusively
proves that lower doses of radiation cause cancer - However, for regulatory purposes, the NRC assumes
that even small exposures to radiation carry some
risk of causing cancer, and that this risk is
linear below 50 rem (50,000 mrem)
40Biological Effects to Typical Occupational
Exposures
- From NRC Regulatory Guide 8.29
- The risk of developing a fatal cancer per 1 rem
(1,000 mrem) of exposure received is assumed to
be about 1 in 2,500 (0.04) - Approximately 1 in 5 adults (20) normally die
from cancer from all possible causes (smoking,
food, drugs, pollutants, genetic traits, etc.) - Therefore, working with radiation may increase
your risk of dying of cancer from 20 (no
occupational radiation exposure) to 20.04 (1 rem
total lifetime occupational radiation exposure)
41Estimated Loss of Life Expectancy from Health
Risks
- Health Risk Estimate of Life
Expectancy Lost - Smoking 1 pack cigarettes per day 6 years
- Being 15 overweight 2 years
- Alcohol consumption 1 year
- Being in any accident 1 year
- Natural hazards 7 days
- Medical radiation 6 days
- Occupational radiation exposure
- 300 mrem/year from age 18 to 65 15 days
- 1000 mrem/year from age 18 to 65 51 days
- Adapted from B.L. Cohen and I.S. Lee, Catalog
of Risks Extended and Updated, Health Physics,
Vol. 61, September 1991.
42Biological Effects to Very High Levels of
Radiation Exposure
- For a single exposure to extremely high levels
of radiation (gt50 rem), the following sequence of
events may occur - Latent period - time lag between the radiation
event and the first detectable effect - Period of demonstrable effects on cells and
tissues - discrete effects of radiation exposure
may be observed - Recovery period - apparent in short-term (days to
weeks) effects. May not occur for some residual
damage, giving rise to long-term effects
43Acute Biological Effects to Very High Levels of
Exposure
- Common Symptoms 50 rem
(50,000 mrem) - Nausea and vomiting, malaise and fatigue,
increased temperature, blood changes - Hemopoietic Syndrome 200 rem (200,000 mrem)
- Ablation of bone marrow, death within months, if
untreated - Gastrointestinal Syndrome 1000 rem (1,000,000
mrem) - Desquamation of intestinal epithelium, death
within weeks, if untreated - CNS Syndrome 2000 rem
(2,000,000 mrem) - Unconsciousness within minutes, death within
days, if untreated - By comparison, the highest exposure at PSU last
year was approximately 0.1 rem above natural
background
445. Radiation Safety
45Radiation Safety
- ALARA
- Program developed in order to keep doses As Low
As is Reasonably Achievable - Obtaining higher doses in order to get an
experiment done quicker is NOT reasonable! - Three main ways to keep your doses ALARA time,
distance and shielding - Ask the RSO for assistance in developing
procedures that help keep your doses ALARA.
46Time, Distance and Shielding
- Minimize your exposure time
- Dry runs (without radioactive material)
- Identify portions of the experiment that can be
altered in order to decrease exposure times. - Make sure you have all necessary equipment
- Maximize distance - Inverse square law
- Doubling distance from source, decreases dose by
factor of four - Tripling it decreases dose nine-fold
- Use appropriate shielding
47Shielding
- High-energy beta emitters (P-32)
- Plexiglas (acrylic) shielding
- Do not use only thin lead to shield beta emitters
- production of bremsstrahlung x-rays
- low-energy x-rays produced by beta interaction
with a high-Z nucleus - Can shield with Plexiglas first, then with lead
on the outside - Gamma emitters (I-125, Cr-51)
- Lead or leaded acrylic
- Neutrons
- hydrogenous material water, concrete
48Contamination Surveys
- Required after EVERY use of unsealed radioactive
materials - If you dont have time to survey, you
dont have time to do your experiment! - Survey yourself, your benchtop, the floor, the
non-radioactive trash and any other area that
could potentially become contaminated - Use the appropriate instrument for the
radionuclide you are using - Use the data on the next slide as a guide
49What Instrument Should I Use?
- H-3 - always use Liquid Scintillation Counter
(LSC) wipe tests - C-14, S-35 and P-33 - both LSC wipe tests and a
Pancake GM probe - P-32 - Pancake GM probe (NaI probe and/or LSC
may also be used) - I-125 - NaI probe (LSC or Gamma counter may also
be used) - Use LSC wipe tests to differentiate between fixed
and removable contamination
50Activity Calculations
Efficiency cpm / dpm dpm cpm / Efficiency If
we detect 2,200 cpm of P-33 with a Pancake GM
probe, we can determine the activity. The
efficiency for P-33 with a Pancake GM probe is
about 10 . dpm 2,200 cpm / 0.10 22,000 dpm
2.2 x 104 dpm We already know that 1 Ci 2.22 x
1012 dpm. 2.2 x 104 dpm x (1 Ci / 2.2 x 1012 dpm)
1 x 10-8 Ci 1 x10-8 Ci x (106 ?Ci / Ci) 1
x102 ? Ci 0.01 ? Ci
51Activity Calculations
- Your laboratorys survey meter is calibrated for
C-14/S-35, P-32 and/or I-125 - A Conversion factor is listed on the meters
calibration sticker this conversion factor is
the inverse of the efficiency. - If you detect 10,000 cpm of P-32 with a pancake
GM probe, and have a conversion factor of 2.2 - cpm x conversion factor dpm
- 10,000 cpm x 2.2 dpm/cpm 22,000 dpm P-32
52Dose Limits
- Federal, state and University regulations limit
the amount of radiation dose allowed to adult and
minor radiation workers, members of the public,
and the fetus of a declared pregnant radiation
worker due to University operations.
53Dose Limits
Adult Occupational Limit 5000 mrem (5.0 rem) /
year Minor Occupational Limit 500 mrem (0.5
rem) / year Member of the Public 100 mrem (0.1
rem) / year Declared Pregnant Radiation Workers
Fetus 500 mrem (0.5 rem) / pregnancy term
54Declared Pregnant Worker
- It is important to note that a woman is
considered pregnant (for NRC license purposes)
ONLY IF SHE DECLARES HERSELF SO, IN WRITING, TO
THE RADIATION SAFETY OFFICER. - A woman may declare or undeclare her pregnancy at
any time it must be in writing to the Radiation
Safety Officer. - For more information, see NRC Regulatory Guide
8.13 - Instruction Concerning Prenatal Radiation
Exposure http//www.nrc.gov/NRC/RG/08/08-013.pdf
55Dose Determination TLDs - Who Needs Them?
- Thermoluminescent dosimeters (TLDs)
- Anyone likely to receive at least 10 of the
limits - Anyone using greater than 1 mCi-hr/week of P-32,
or gt 0.1 mCi-hr/week of gamma emitters - Anyone working at the Breazeale Nuclear Reactor
- Anyone performing radioiodinations
- Anyone working with x-ray machines
- If working with sources gt100 mrem/hr at 1 foot
- NOT assigned to anyone working exclusively with
H-3, C-14, S-35, Ca-45 and / or P-33
56Dose Determination Bioassays - Who Needs Them?
- Bioassays are required of
- Anyone performing radioiodinations
- Anyone using greater than 100 mCi of H-3 at any
one time
576. Procedures
58Radioactive Material Orders
- Must be approved by the RSO before being placed
59Incoming Packages
- Must be checked as outlined in the radiation
safety manual, Appendix 4. Only authorized users
as listed on the license may receive packages. - After removing the radioactive material, all
radioactive markings on the package must be
removed or defaced prior to placing the package
for disposal or recycling.
60Inventory Forms
- Must be filled out and returned to the RSO in
order for the supervisor to receive credit for
disposal of the material - Supervisors are considered to be in possession of
each isotope order until EHS receives the
inventory form - This could lead to EHS denying a request for a
radioactive material order if it causes the
supervisor to exceed their possession limit
61Radioactive Material Transfers
- Any radioactive material transfers between lab
groups must be approved by the RSO. - Shipments to other facilities require approval by
the RSO and must comply with all shipping
regulations. - Radioactive materials may not be carried between
the two science buildings.
62Authorizations
- Authorizations for radioactive material usage
must be approved by the RSO. - No supervisor will be permitted to receive an
amount of radioactive material that will cause
him or her to have in excess of their allowed
possession limit.
63Security
- All radioactive materials, including radioactive
waste, must be secured when unattended, even if
for a very short time - This can be accomplished by keeping the
radioisotope lab door locked at all times.
647. Radioactive Waste
65Solid Radioactive Waste
- Separated by nuclide
- Only in marked containers in the radioisotope
lab. - No liquids (5 mL or less per container)
- Record, survey and dispose of material (half-life
lt120 days) as detailed in the Radiation Safety
Manual, appendix 8. - Decay a minimum of 10 half-lives. Obliterate all
rad labels and dispose of in regular trash. - Keep same nuclide of different reference dates
separated. - For EPA Hazardous materials, contact the RSO for
instructions
66Liquid Radioactive Waste
- Separated by nuclide
- Only in marked containers in the radioisotope
lab. - No solids (except for 1 or 2 pH strips)
- pH must be between 5 and 9
- If biohazard, add 10 bleach before adding rad
waste - EPA Hazardous waste must be separated from
non-hazardous radioactive waste - Record, survey and dispose of material (half-life
lt120 days) as detailed in the Radiation Safety
Manual, appendix 8. - Decay a minimum of 10 half-lives can then wash
down sink. - Keep same nuclide of different reference dates
separated.
678. Major Spill Response
68Major Spill Response Procedure
- No matter how careful we are, we are all
sometimes still vulnerable to having an accident.
On the following slides are the steps to take if
a major spill occurs. Follow this general
procedure.
69Major Spill Response Procedure
- Immediately notify the RSO (Jill Keeney) or
Science Safety Director (Roy Nagle) and the
Laboratory Supervisor. - 1. Stop the spread of radioactive material. If
there is any sign of hallway contamination, run a
rope across the hall at least 10 feet from the
door on both sides of the lab. Use Caution
signs and duct tape. Enforce the no-pass rule,
station someone to stop traffic.
70Major Spill Response Procedure
- 2. Warn others in laboratory. Lock and post a
notice on the radioisotope lab door. Survey self
and shoes-cover shoes with plastic bags if shoes
are contaminated. This will help minimize the
spread of the contamination.
71Major Spill Response Procedure
- 3. Survey all lab personnel. Record results
(Fred left shoe 10,000 cpm-GM at 1 cm, Betty
palm of right hand 950 cpm-GM at 1 cm). Pay
particular attention to skin contamination.
Although unlikely, skin dose may be a problem.
Document levels prior to a quick clean,
recheck/re-document.
72Major Spill Response Procedure
- 4. Survey people in other labs if there is any
indication of widespread problems. If it appears
radioactivity may be widespread, the RSO or
Safety officer will survey other labs.
73Major Spill Response Procedure
- 5. Call in Help. The laboratory supervisor
should be present to organize the cleanup. The
supervisor should call in all staff and students. - Request help for cleanup from the RSO and Science
Safety Officer.
74Major Spill Response Procedure
- 6. Determine if the chemical composition of the
spill could cause airborne particulate
contamination if the spill was allowed to dry.
If so, mop immediately.
75Major Spill Response Procedure
- 7. Establish a 'Clean' area. The area should be
inside the room if possible, in the hallway if
not. Issue boots or plastic bags for shoe
covers. Absorbent bench paper is handy for
covering floors to use as a clean area.
76Major Spill Response Procedure
- 8. Survey public areas. Have someone with clean
feet survey hall, elevator, stairs, etc. - If wider contamination is found, expand your
roped - off area.
77Major Spill Response Procedure
- 9. Survey the room. Remove people from lab until
a survey of the room is performed. Smears are
not necessary, but documentation is required.
78Major Spill Response Procedure
- 10. Assign some lab personnel to cleaning the
halls while others continue to survey. Extend
roped off area as necessary. Do not permit lab
personnel to decontaminate their own space until
all public areas are clean.
79Major Spills - Other Cautions
- 1. Enforce glove changes whenever a glove gets
contaminated. - 2. Work from cleaner areas towards areas with
more contamination. - 3. Do not permit removal of contaminated shoes.
People tend to contaminate their socks, then
their feet. Have personnel place plastic bags
over their shoes and walk carefully. - 4. If the room has to be roped off and not used
until the next day, NRC notification may be
required.
809. Laboratory Rules
81Radionuclide Laboratory Rules
- 1. Liquid Radioactive materials may only be
possessed or used within the radioisotope lab in
VLCS.
82Radionuclide Laboratory Rules
- 2. Persons working in radionuclide laboratories
must be familiar with regulations and radiation
safety procedures. New personnel are required to
have safety instruction before beginning work
with radioactive materials.
83Radionuclide Laboratory Rules
- 3. Orders for shipment of radioactive materials
to and from the University and transfers between
supervisors within the University must be
processed through the RSO.
84Radionuclide Laboratory Rules
- 4. Inventory forms for radioactive materials must
be kept current and according to procedures
detailed in the Radiation Safety Manual, Appendix
8.
85Radionuclide Laboratory Rules
- 5. People using radioactive materials are
responsible for conducting routine surveys to
detect excessive contamination or radiation
levels each time unsealed radioactive materials
are used. Procedures are detailed in Appendix 5
of the Radiation Safety Manual.
86Radionuclide Laboratory Rules
- 6. People using radioactive materials are
responsible for the immediate decontamination of
facilities that become contaminated in excess of
allowed levels.
87Radionuclide Laboratory Rules
- 7. Pipetting by mouth is prohibited in
laboratories where unsealed radioactive materials
are used.
88Radionuclide Laboratory Rules
- 8. Persons working with unsealed radioactive
material must wear laboratory coats, or other
protective clothing and appropriate protective
gloves.
89Radionuclide Laboratory Rules
- 9. Eating, drinking, or the storage of food or
beverages is prohibited in the radioisotope lab.
90Radionuclide Laboratory Rules
- 10. Radioactive materials must be discarded only
into appropriately labeled radioactive waste
containers.
91Radionuclide Laboratory Rules
- 11. All containers of radioactive material must
be labeled with the radiation caution symbol,
the users name, the radionuclide, the activity
and the date. Lead shields, cabinets,
refrigerators and other storage areas for
radioactive material must also be conspicuously
labeled.
92Radionuclide Laboratory Rules
- 12. Licensed radioactive material in storage must
be secure from unauthorized removal or access.
Radioactive material not in storage must be
controlled and under constant surveillance.
93Violations
- Immediate suspension for
- Radioactive materials in the regular trash
- Eating, drinking, smoking or storage of food
in a posted lab or area - In case of immediate suspensions
- All persons working under the supervisor, or
in the supervisors lab, must stop using
radioactive materials immediately - Authorization is suspended until further notice
94Should you have any questions,
Roy Nagel Science Safety Officer Ext.
nagel_at_juniata.edu
Jill Keeney Radiation Safety Officer Ext.
3577 keeney_at_juniata.edu
- A hard copy of the Radiation Safety Manual is
located in the radioisotope lab in VLCS. - An electronic copy and this power point file is
on the P drive at P\Keeney\P radiation safety