WEBSITE

1
ORGANIC CHEMISTRY LAB II CHEM 334

• WEBSITE
• http//www.uccs.edu/laugenst/chem334/index.htm

2
SYLLABUS

• Goals
• Typical lab
• Lab notebook
• Lab reports
• Quizzes exams
• Late lab reports
• Missed labs

• Work efficiently
• Academic policies
• Grading
• Resources
• Disabilities
• Clickers

3
SCHEDULE

• Links to powerpoint slides and report forms

4
LAB NOTEBOOK

• Notebook Preparation
• Before lab
• Title
• Purpose
• Reference to procedure
• Changes to referenced procedure
• Balanced reaction mechanism
• Table of reagents
• Relevant physical properties, amounts, hazards
• Calculate limiting reagent
• Flow chart

5
LAB NOTEBOOK

• During Lab
• Record data
• Amounts actually used, times, temperatures,
  results, etc.
• Record all observations
• Expected unexpected, impacts on yield purity

6
LAB NOTEBOOK

• After Lab
• Record post-lab results, physical properties, TLC
  data, spectroscopic data, etc.
• Calculate theoretical and yield.
• Calculate error of physical properties.
• Identify unknowns with name and structure.

7
LAB REPORT

• Formatted reports
• Link from schedule
• Typed
• Computer drawn structures
• Turn in completed report form, copies of notebook
  pages, TLC plates, spectra, etc.
• Due 1 week after completion of experiment

8
WEEK 1

• Check in
• Safety
• Scavenger Hunt Redux

9
Methyl benzoate
10
overtones
sp2 C-H
CC
CO
C-O
OOP
11
(No Transcript)