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CHEE 209 Analysis of Process Data

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Fitting empirical models between reactor temperature and product yield ... Used to assist in decision making (statistics doesn't replace sound engineering ... – PowerPoint PPT presentation

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Title: CHEE 209 Analysis of Process Data


1
CHEE 209Analysis of Process Data
  • Tom Harris
  • Fall 2009

The original compilation of these notes by Prof.
Kim McAuley
2
Role of Statistical Methods
  • Summarizing data
  • using a few key numbers or graphs
  • uncover or reveal complex patterns
  • Decision-making in the presence of uncertainty
  • Has the concentration of a contaminant in an
    effluent stream changed appreciably?
  • Has the quality of our polyurethane foam
    improved?
  • Is the quality of a mineral deposit sufficient
    to justify investments?
  • Use confidence limits and hypothesis tests and
    control charts to find answers to these
    questions.

3
Role of Statistical Methods
  • 3. Identifying relationships in data
  • Designing experiments to uncover relationships
    among variables,
  • Fitting empirical models between reactor
    temperature and product yield
  • Development of calibration methods for chemical
    property analysis
  • Test suitability of various models

4
Why do need statistical methods?
  • Presence of Process or Inherent Variability
  • Price of Platinum
  • Temperature Measurements
  • Moisture Content of a Paper Product

5
Sources of Process Variability
  • instrumentation and measurements
  • operator interventions
  • disturbances
  • from raw materials or upstream units
  • Temperature or composition of feed stream
  • ambient conditions
  • Air temperature
  • Cooling water temperature
  • external factors demand, speculation

6
Types of Data
  • Discrete
  • number of defective items, number of people
  • colours
  • taste
  • Continuous
  • temperature
  • pressure
  • composition

Combination discrete continuous
7
Types of Data
  • May be collected with respect to time, i.e.
    composition measurements every hour, minute or
    second
  • Spatial component
  • Collected with respect to distance
  • 2 or 3 D

8
Data Collection
  • Passive Collection
  • record results without actively intervening in
    the operation of the process
  • historical databases of operational or
    geophysical data
  • Active Collection Intervention
  • do a planned experiment
  • guarantees a cause and effect relationship
  • Example police officers and crime

9
Value of statistical methods
  • Established body of both theory practice that
    provides a scientific systematic approach for
  • collection of data
  • methods for analysis and interpretation
  • Used to assist in decision making (statistics
    doesnt replace sound engineering judgment and
    knowledge)
  • Universal language that transcends specific
    disciplines, i.e. engineering, business, law,
    medicine

10
Course Overview
  • describing data
  • describing variability
  • probability
  • decision-making in the presence of uncertainty
  • hypothesis tests and confidence intervals
  • statistical quality control
  • empirical modeling
  • linear regression

Examples from chemical engineering, chemistry
geosciences
11
Course Objectives
  • Understand motivation for use of statistics
  • Proficient and confident in using a number of
    introductory techniques using hand and
    computer-based calculations
  • Develop a critical awareness regarding
    statistical thinking which is important for
    your responsibilities as engineers and citizens.
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