CombeChem elab book UI

1
CombeChem elab book UI

• Draft proposed by m.c. schraefel, june 15 03
• Revised, June 19, 03
• Based on tea experiment runs 1 and 2

2
Lab Bench Station
Chemist
Date

PLEASE ENTER YOUR ID(iButton) to begin
loggingfor your experiment(s)
3
(screen 2a)
Tea 1a Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1a)
Chemist Graham
Date
Friday, July 13, 2003
Cancel
Pause
4
(screen 2a1)
Tea 1a Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1a)
Chemist Graham
Date
Friday, July 13, 2003
Cancel
Pause
5
(screen 2b)
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml ____
Weights Planned Actual Tea
20g 20.50g
Record
Yield _______ Tea _______ml ID Location
ProcessOverview

• Phase 1 Make Tea -
• Phase 2 Decant Tea -

DataOverview
Cancel
Pause
Log Out
6
(screen 3)
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 10_ml
Weights Planned Actual Tea
20g 20.50g
Record
Yield Tea _______
Yield _______ Tea _______ml ID
Location
ProcessOverview

• Phase 1 Make Tea -
• Phase 2 Decant Tea -

DataOverview
Cancel
Pause
Log Out
7
(screen 4)
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set
Yield _______ Tea _______ml ID
Location
ProcessOverview
TLC captures (link)

• Phase 1 Make Tea -
• Phase 2 Decant Tea -

DataOverview
Cancel
Pause
Log Out
8
(screen 5)
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set

• Make Tea
• Apparatus
• boiling thingy
• Round bottomed thing for water
• Flute that goes into round thing
• Syringe
• TLC

Yield Tea _______

• Method
• bring water to boil
• Add tea
• Reflux for 5 mins
• Sample 1/min
• Assess by color and aroma
• decant

ProcessOverview

• Phase 1 Make Tea -
• Phase 2 Decant Tea -

Sample at ______ (min). State is _________
Sample at ______ (min). State is
_________ Sample at ______ (min). State is
_________ Sample at ______ (min). State is
_________ Sample at ______ (min). State is
_________
Record
Done
DataOverview
Actual time for completion ______
Record
Cancel
Pause
Log Out
9
(screen 6)
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set

• Make Tea
• Apparatus
• boiling thingy
• Round bottomed thing for water
• Flute that goes into round thing
• Syringe
• TLC

Yield Tea _______

• Method
• bring water to boil
• Add tea
• Reflux for 5 mins
• Sample 1/min
• Assess by color and aroma
• decant

TLC captures (link)
ProcessOverview

• Phase 1 Make Tea
• Phase 2 Decant Tea

Sample at ____ (min). State is _________
Sample at ______ (min). State is
_________ Sample at ______ (min). State is
_________ Sample at ______ (min). State is
_________ Sample at ______ (min). State is
_________
Record
Done
DataOverview
Actual time for completion ______
Record
Cancel
Pause
Log Out
10
(screen 6b)
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set

• Make Tea
• Apparatus
• boiling thingy
• Round bottomed thing for water
• Flute that goes into round thing
• Syringe
• TLC

Yield Tea _______

• Method
• bring water to boil
• Add tea
• Reflux for 5 mins
• Sample 1/min
• Assess by color and aroma
• decant

TLC captures (link)
ProcessOverview

• Phase 1 Make Tea
• Phase 2 Decant Tea -

Sample at __1.2_ (min). State is ______
Sample at ______ (min). State is
_________ Sample at ______ (min). State is
_________ Sample at ______ (min). State is
_________ Sample at ______ (min). State is
_________
Record
Done
DataOverview
Actual time for completion ______
Record
Cancel
Pause
Log Out
11
(screen 6c)
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set

• Make Tea
• Apparatus
• boiling thingy
• Round bottomed thing for water
• Flute that goes into round thing
• Syringe
• TLC

Yield Tea _______

• Method
• bring water to boil
• Add tea
• Reflux for 5 mins
• Sample 1/min
• Assess by color and aroma
• decant

TLC captures (link)
ProcessOverview

• Phase 1 Make Tea
• Phase 2 Decant Tea-

Sample at __1.2_ (min). State is __30____
Sample at ______ (min). State is
_________ Sample at ______ (min). State is
_________ Sample at ______ (min). State is
_________ Sample at ______ (min). State is
_________
Set
Record
Done
DataOverview
Actual time for completion ______
Record
Cancel
Pause
Log Out
12
(screen 6d)
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set

• Make Tea
• Apparatus
• boiling thingy
• Round bottomed thing for water
• Flute that goes into round thing
• Syringe
• TLC

Yield Tea _______

• Method
• bring water to boil
• Add tea
• Reflux for 5 mins
• Sample 1/min
• Assess by color and aroma
• decant

TLC captures (link)
ProcessOverview

• Phase 1 Make Tea
• Phase 2 Decant Tea -

Sample at __1.2_ (min). State is __30____
Sample at __2.5_ (min). State is
__60_____ Sample at __4___ (min). State is
_100____
Set
Set
Complete
Set
DataOverview
Actual time for completion __4min_
Record
Cancel
Pause
Log Out
13
(screen 6e - alternate)
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set

• Make Tea
• Apparatus
• boiling thingy
• Round bottomed thing for water
• Flute that goes into round thing
• Syringe
• TLC

Yield Tea _______

• Method
• bring water to boil
• Add tea
• Reflux for 5 mins
• Sample 1/min
• Assess by color and aroma
• decant

TLC captures (link)
ProcessOverview

• Phase 1 Make Tea -
• Phase 2 Decant Tea -

Sample at __1.2_ (min). State is __30____
Sample at __2.5_ (min). State is
__60_____ Sample at __4___ (min). State is
_100____
Set
Set
Complete
Set
DataOverview
Actual time for completion __4min_
Record
Cancel
Pause
Log Out
14
(screen 6e - alternate)
Tea 1 Water 1 Light 4
Phase Name
Experiment Selected

LogBench Station Active
(Tea 1)
Chemist Graham
Process Template Selection List
Date
Friday, July 13, 2003
Method _
X
Process.something something Process.some
thing something Process.something
something Process.something
something Process.something something
Apparatus_
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set

• Make Tea
• Apparatus
• boiling thingy
• Round bottomed thing for water
• Flute that goes into round thing
• Syringe
• TLC

Yield Tea _______

• Method
• bring water to boil
• Add tea
• Reflux for 5 mins
• Sample 1/min
• Assess by color and aroma
• decant

TLC captures (link)
ProcessOverview

• Phase 1 Make Tea -
• Phase 2 Decant Tea -

Sample at __1.2_ (min). State is __30____
Sample at __2.5_ (min). State is
__60_____ Sample at __4___ (min). State is
_100____
Set
Set
Complete
Set
DataOverview
Actual time for completion __4min_
Record
Cancel
Pause
Log Out
15
(screen 6e)
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set

• Make Tea
• Apparatus
• boiling thingy
• Round bottomed thing for water
• Flute that goes into round thing
• Syringe
• TLC

Yield Tea _______

• Method
• bring water to boil
• Add tea
• Reflux for 5 mins
• Sample 1/min
• Assess by color and aroma
• decant

TLC captures (link)
ProcessOverview

• Phase 1 Make Tea (complete)
• Phase 2 Decant Tea

Sample at __1.2_ (min). State is __30____
Sample at __2.5_ (min). State is
__60_____ Sample at __4___ (min). State is
_100____
Set
Set
Complete
Set
DataOverview
Actual time for completion __4min_
Record
Cancel
Pause
Log Out
16
(screen 7)
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set

• Decant Tea
• Apparatus
• Big flask
• funnel
• Filter paper

Yield Tea _______

• Method
• Cool tea liquid
• Pour through filter paper
• Measure resulting yield
• Store result

TLC captures (link)
ProcessOverview

• Phase 1 Make Tea
  (complete)
• Phase 2 Decant Tea -

Record
Yield ________ Amount of material_______ml
Note
Record
Note
DataOverview
Cancel
Pause
Log Out
17
(screen 7b)
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set

• Decant Tea
• Apparatus
• Big flask
• funnel
• Filter paper

Yield Tea _______

• Method
• Cool tea liquid
• Pour through filter paper
• Measure resulting yield
• Store result

TLC captures (link)
ProcessOverview

• Phase 1 Make Tea (complete)
• Phase 2 Decant Tea -

Yield ________ Amount of material_______ml
Note
Record
Note
Record
DataOverview
Cancel
Pause
Log Out
18
(screen 7c)
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set
Yield Note (1) Date Friday, July 13, 2003, 1445
GMT Due to failure with filtration paper, we
were unable to derive more than 90 yield of the
material. Next time, Id like to use a different
method for decanting - one that avoids filter
paper. -------------------------- Yield Note
(2) Date Friday, July 13, 2003, 1448 GMT An
earnest student, attempting to help clean up
has just destroyed the filter papers.
Cancel Save X

• Decant Tea
• Apparatus
• Big flask
• funnel
• Filter paper

Yield Tea _______

• Method
• Cool tea liquid
• Pour through filter paper
• Measure resulting yield
• Store result

TLC captures (link)
ProcessOverview

• Phase 1 Make Tea (complete)
• Phase 2 Decant Tea

Yield 90 Amount of material_______ml
Note
Set
Note
Record
DataOverview
Cancel
Pause
Log Out
19
(screen 7d)
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set

• Decant Tea
• Apparatus
• Big flask
• funnel
• Filter paper

Yield Tea _______

• Method
• Cool tea liquid
• Pour through filter paper
• Measure resulting yield
• Store result

TLC captures (link)
ProcessOverview

• Phase 1 Make Tea (complete)
• Phase 2 Decant Tea -

Yield 90 Amount of material_900_ml
Note
Set
Note
Record
DataOverview
Cancel
Pause
Log Out
20
(screen 7d)
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set

• Decant Tea
• Apparatus
• Big flask
• funnel
• Filter paper

Yield Tea _______

• Method
• Cool tea liquid
• Pour through filter paper
• Measure resulting yield
• Store result

TLC captures (link)
ProcessOverview

• Phase 1 Make Tea (complete)
• Phase 2 Decant Tea

Yield 90 Amount of material_900_ml
Note
Set
Note
Set
DataOverview
Decant Tea
complete
additional
Cancel
Pause
Log Out
21
(screen 7e)
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set

• Decant Tea
• Apparatus
• Big flask
• funnel
• Filter paper

Yield Tea _______

• Method
• Cool tea liquid
• Pour through filter paper
• Measure resulting yield
• Store result

TLC captures (link)
ProcessOverview

• Phase 1 Make Tea
  (complete)
• Phase 2 Decant Tea
• (complete)

Yield 90 Amount of material_900_ml
Note
Set
Note
Set
DataOverview
DataOverview
Decant Tea Complete
Cancel
Pause
Log Out
22
(screen 8 )
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set
Yield 90 Tea 900 ml ID
(Select Field and Scan code) Location
(Select Location)
ProcessOverview

• Phase 1 Make Tea -
• (complete)
• Phase 2 Decant Tea -
• (complete)

TLC captures (use scan station)
DataOverview
Cancel
Pause
Log Out
23
(screen 9 )
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set
Yield 90 Tea 900 ml ID
(Select Field and Scan code) Location
(Select Location)
ProcessOverview

• Phase 1 Make Tea -
• (complete)
• Phase 2 Decant Tea -
• (complete)

TLC captures (use scan station)
DataOverview
Cancel
Pause
Log Out
24
(screen 10 )
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set
Yield 90 Tea 900 ml ID
(689 4893
485) Location
TLC captures (link)
ProcessOverview
Freezer 1, Room 290 Freezer 2, Room 290 Freezer
3, Room 245

• Phase 1 Make Tea -
• (complete)
• Phase 2 Decant Tea -
• (complete)

TLC captures (use scan station)
DataOverview
Cancel
Pause
Log Out
25
(screen 11 )
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set
Yield 90 Tea 900 ml ID
(689 4893
485) Location
ProcessOverview
Freezer 1, Room 290

• Phase 1 Make Tea -
• (complete)
• Phase 2 Decant Tea -
• (complete)

TLC captures (use scanner)
DataOverview
Cancel
Pause
Log Out
26
(screen 12 )
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set
Yield 90 Tea 900 ml ID
(689 4893
485) Location
ProcessOverview
Freezer 1, Room 290

• Phase 1 Make Tea -
• (complete)
• Phase 2 Decant Tea -
• (complete)

TLC captures Tea1 TLC link
Exp Tea1 Data Capture Concluded at
DataOverview
Time Stamp
Cancel
Pause
Log Out
27
(screen 12b )
Tea 1 Water 1 Light 4
Experiment Selected
LogBench Station Active
(Tea 1)
Chemist Graham
Date
Friday, July 13, 2003
Measures Planned Actual Water
1000ml 1001ml
Weights Planned Actual Tea
20g 20.50g
Measure Set
Yield 90 Tea 900 ml ID
(689 4893
485) Location
ProcessOverview
Freezer 1, Room 290

• Phase 1 Make Tea -
• (complete)
• Phase 2 Decant Tea -
• (complete)

TLC captures Tea1 TLC link
Exp Tea1 Data Capture Concluded at
DataOverview
Time Stamp
Cancel
Pause
Log Out
28
LogBook Station
Chemist
Date

PLEASE ENTER YOUR ID(iButton) to begin
loggingfor your experiment(s)
29
(screen 13 - alternate )
LogBook Station
Chemist
Date
You have been successfully logged out of the
LogBookstation, Graham. TLC and Compound ID
remain to be done for Tea1 A note has been
mailed to your logbook as a reminder.
Cancel
Pause
Log Out