??e???? ?a? ??a???

1
??e???? ?a? ??a???ß?s? e??p??sµ?? e??ast?????
?µe??da t?? ???? µe ??µa
????d?? de??µat?????a? de??µ?t?? ?d?t?? ?a?
t??f?µ?? ??a µ????ß???????? ?a? ??µ??? ??e???
?e?te?e? µe??d?????e? st?? ???ast???a?? ??µ?s?a
??e?a

• ?. Te?f????
• ?. ?a???s??

????a, 22 ??eµß???? 2013
2
????t?ta ?a? a???p?st?a ap?te??sµat?? d???µ??
????? e??at?stas?? ?a? pe??ßa????t???? s?????e?
de??µat?????a
a?a??t??
de??µa e??ast?????
ap?t??esµa
?e???sµ?? a?t??e?µ???? d???µ??
µ???d?? d???µ??
e??p??sµ??
3
d?asf???s? p???t?ta? ap?te?esµ?t??

• efa?µ??? t?? d?e????? p??t?p?? ISO 17025
• pe????e? ??e? t?? apa?t?se?? p?? p??pe? ?a
  ??a??p????? ta e??ast???a d???µ?? ?a?
  d?a???ß?se?? s?µpe???aµßa??µ???? t??
  de??µat?????a?, p???e?µ???? ?a ap?de????? ?t?
• ????? t? d??at?t?ta ?a pa??????
  te?????? ?????a ap?te??sµata

a?t? t? d?e???? p??t?p? ???s?µ?p??e?ta? ap? t???
f??e?? a???????s?? ?? ß?s? ??a t?? d?ap?ste?se??
p?? ???????? sta e??ast???a d???µ?? ?a?
d?a???ß?se??
4
?e?t???? ???ast???? ??µ?s?a? ??e?a?

• ??ap?ste?µ??? e??ast???? ap? t? ?????? S?st?µa
  ??ap?ste?s??/ ?????? S?st?µa
  ?p?d?µ?? ????t?ta? (?S??/?S??) ap? t? 2005
• a???µ?? p?st?p???t???? d?ap?ste?s?? 213
• ??e? ep?s?µ? a?a?????s? ??a t?? ????t?ta t??
  ap?te?esµ?t?? p?? pa???e?

5
e??a? ?p???e?t???? ? ??e???? ?a? ? d?a???ß?s? t??
e??p??sµ??

• pe???aµß??eta? st? p??t?p? ISO 17025 ??
  te????? apa?t?s? ??a ta e??ast???a

? e??p??sµ?? e??a? ??a? ap? t??? pa?????te? p??
µp??e? ?a ep??e?se? t? ap?t??esµa t?? d???µ??
6
apa?t?se?? t?? p??t?p?? ISO 17025 ??a t??
e??p??sµ?

• µ???s?µa?t? ??d???p???s?
• ???s? ap? e???s??d?t?µ??? p??s?p???
• e??µe??µ??e? ?d???e? ???s?? e????a
• d?a??s?µe?
• t???s? a??e???
• ??e???? ?a? d?a???ß?s?
• ?? µ???? t?? s?st?µat?? p???t?ta? p??
  efa?µ??e?, t? e??ast???? p??pe? ?a d?a??te? ??a
  te?µ????µ??? p????aµµa ??a t?? ??e??? ?a? t??
  d?a???ß?s? t?? e??p??sµ?? p?? ???s?µ?p??e?

7
??e???? ?a? d?a???ß?s? t?? e??p??sµ??(1)
?a?a??sµ?? ?a? ap???µa?s?
s??t???s?
??e???? ?a??? ?e?t?????a?
d?a???ß?s?
d?asf???s? t?? p???t?ta? t?? ap?te?esµ?t??
8
??e???? ?a? d?a???ß?s? t?? e??p??sµ?? (2)

• ???e p?te
• ?a?????eta? ap? t? e??ast????, a?????a µe t??
  t?p? ?a? t? sta?e??t?ta t?? e??p??sµ??, t?
  s????t?ta ???s??, t?? ?d???e? t?? ?atas?e?ast?
  ?a? t?? ?ate????t???e? ?d???e? d?e????
  a?a?????sµ???? ???a??sµ?? (p.?. EA, UKAS)

s??ta?? d?ad??as??? ?a? ?d????? e??as?a?
de? ?p???e? ?e????? ?a???a? s?et??? µe ta
d?ast?µata e?????? d?a???ß?s??. ???e pe??pt?s?
??????? µet??se?? p??pe? ?a e?et??eta? ?e????st?

9
??e????/d?a???ß?s? p???? e??p??sµ? af???

• ??a???ß?s?

• ?dat????t?a, ep?ast????? ???ß?????, a?t??a?sta,
  ?µ??e??p???t??, ???e?a, ?ata???e??
• µet??t??? ???a?a ?e?µ?µet?a, ?????µet?a, ??????,
  pe??µet?a, ?ataµet??t?? ap??????
• ????µet???? e??p??sµ? p?p?te?, a?t?µat???
  d?a?eµ?t??
• ß????t??? e??p??sµ? s?s?e??? d????s??, ???????
  e??p??sµ?

a?t?? t?? e??p??sµ? p?? µp??e? ?a ap?te??se?
s?µa?t??? p??? aßeßa??t?ta? st? te???? ap?t??esµa
t?? d???µ??
??e? ep?d?as? sta ap?te??sµata
10
t? s?µa??e? d?a???ß?s? t?? e??p??sµ???

• s?????s? t?? e?de??e?? µ?t??s?? p?? d??e? t?
  ???a?? µe t?? a?t?st???e? e?de??e?? e??? p??t?p??
  a?af????

• d?????s? st?? e?de??e?? t?? ???????
• ?p?????sµ?? aßeßa??t?ta? µ?t??s??

s???p??????eta? st?? s??????? aßeßa??t?ta t??
ap?te??sµat??
11
?d??t?te? p??t?p?? a?af????

• ?a ??e? a???ße?a t??????st?? 3 f???? ?a??te?? ap?
  t? ???a?? ?p? d?a???ß?s?
• ?a ??e? ?????as?µ?t?ta sta d?e??? p??t?pa µ?t??s??

p.? ??a ta p??t?pa µ?t??s?? ?e?µ???as?a? e??a? ?
??a??t?ta ?a s??d?e?? t? ap?t??esµa µ?a? µ?t??s??
µe t?? ??e??? ???µa?a Te?µ???as?a? t?? 1990
(ITS-90)
12
??e???? ???µa?a Te?µ???as?a? t?? 1990
(ITS-90)
?f??? t?? d?a???ß?s? µ??? t?? p??t?p?? ?e?µ?µ?t???
S?µe?a a?af????
13
???aµ?da ?????as?µ?t?ta? ?e?µ???as?a?
14
a???p?st?a ?p??es??? d?a???ß?s??

• e??ast???? d?a???ß?s?? d?ap?ste?µ??? ap? t? ?S??
• a?a?????sµ??? e??ast???? ap? a?t?st???? f???a t??
  e??te?????
• ???????? ??st?t??t? ?et??????a? (???)
  t???s? e?????? p??t?p?? µ?t??s??

ad??spast? a??s?da ?????as?µ?t?ta?
15
pa??de??µa e?????? e??p??sµ??

• 24??? pa?a???????s? (a?? 15) µ?s? as??µat??
  s?st?µat?? ?ata??af?? t?? ?e?µ???as?a? t??
  ?a??µ??
• d??at?t?ta e?d?p???s?? t?? e???s??d?t?µ????
  p??s?p???? µe email/sms se pe??pt?s? pa??????s??
  ap? t?? ?a????sµ??e? a?????

16
pa??de??µa e??? ?a??e??µ???? p?????µµat?? ??a
t?? ??e??? ?a? t?? d?a???ß?s? t?? e??p??sµ?? (1)
e?d?? e??p??sµ?? apa?t?s? p??te???µe?? s????t?ta
ep?ast???? ???ßa??? a) ?a?a??sµ?? ?a? ap???µa?s? es?te????? ep?fa?e??? ß) pa?a???????s? t?? ?e?µ???as?a? ?) sta?e??t?ta ?a? ?µ???µ??f?a ?e?µ???as?a? (a) µ???a?a ß) ?a??µe???? ?) st?? ??a??? ?e?t?????a?, ???e 2 ?????a ?/?a? µet? ap? ep?s?e??/ t??p?p???s?
pH µet?a a) ?a?a??sµ?? ??e?t??d??? ß) ßa?µ???µ?s? µe ???s? ???µ?st???? d?a??µ?t?? ?a??µe????
ta d?ast?µata p??te????ta? ap? t? pa???t?µa t??
EA-4/10 Accreditation in microbiological
laboratories
17
pa??de??µa e??? ?a??e??µ???? p?????µµat?? ??a
t?? ??e??? ?a? t?? d?a???ß?s? t?? e??p??sµ?? (2)
e?d?? e??p??sµ?? apa?t?s? p??te???µe?? s????t?ta
????? a) ?a?a??sµ?? ?a? ap???µa?s? ß) ??e???? ?a??? ?e?t?????a? µe ß???? e??as?a? ?) d?a???ß?s? µe p??t?p? ß???? a) ?p?te apa?te?ta? ?a? µet? ap? ???e ???s? ß) p??? ap? ???e ???s? ?) et?s?a
?dat????t?a a) ?de?asµa , ?a?a??sµ??, ap???µa?s? ?a? epa?ap????s? ß) sta?e??t?ta ?a? ?µ???µ??f?a ?e?µ???as?a? a) µ???a?a ß) et?s?a
?d?a??????? ?e?µ?µet?? a) ??e???? ?a??? ?e?t?????a? ß) d?a???ß?s? a) et?s?a ß) ???e 5 ?????a
ta d?ast?µata p??te????ta? ap? t? pa???t?µa t??
EA-4/10 Accreditation in microbiological
laboratories ?a? t? Lab11/UKAS
18
?a? epe?d? ta µet???????? ?a?a?t???st??? t??
µet??t???? ??????? de? pa?aµ????? aµet?ß??ta se
??? t? d????e?a t?? ???? t???

• e?a?t?a?
• ?atap???se?? ?at? t?? ???s?
• pe??ßa????t???? s???????
• f?s????????? f?????

?a p??pe? ?a e??????ta? ?a? ?a d?a???ß????ta? se
??? t? d????e?a t?? ???? t???
19
?e?te?? µe??d?????a st? ????

• ?SO??????S ???????OS??S

20
t? ???? d?a???ß??e? e??p??sµ? p?? a???e? st??
pa?a??t? ?at?????e?

• ?a??µ??? ?e?µ???as?a? (ep?ast????? ???ß?????,
  ???e?a, ?ata???te?, ?????? ?????? ???ß?????,
  ???t????? ?a??µ??? ?dat????t?a)
• ????µet???? e??p??sµ? (p?p?te? sta?e???/µetaß??t??
  ?????)
• ßa??µet???? e??p??sµ? (a?a??t???? ?????)
• ?e?µ?µet???? e??p??sµ? (p.?. as??µata
  ?ata??af???, ?e?µ?µet?a ?????)

d?asf???s? ?t? ??a??p?????ta? ?? apa?t?se?? t??
p??t?p??
21
d??µe?? e?pa?de?s? p??s?p???? ???? st? ????????
??st?t??t? ?et??????a? (???) (1)

• e?sa??????? ?????e?, d?e???? ???µa?a ?e?µ???as?a?
  ITS90
• µ???d?? d?a???ß?s?? ?e?µ?µ?t??? (?µes??
  a?????s??, d?ast???? ?????, PRTs ?.a.)
• aßeßa??t?te? d?a???ß?s?? ?e?µ?µ?t??? 
• e?sa??????? ?????e? ?a? µ???d?? d?a???ß?s?? ??a
  pe??ßa????t????? ?a??µ??? ?e?µ???as?a?
• e?t?µ?s? aßeßa??t?ta?
• p?a?t??? e??s??s? st? e??ast???? ?e?µ???as?a? t??
  ???

22
d??µe?? e?pa?de?s? p??s?p???? ???? st? ????????
??st?t??t? ?et??????a? (???) (2)

• t? ???? p???? d?a??te? e?pa?de?µ??? p??s?p??? ??a
  t? d?e????e?a es?te????? d?a???ß?se??,
  e???????µ??ta? ?ts? p?????, ded?µ???? ?t? t?
  ??st?? t?? e??te????? e?????? e??a? p??? ?????
  ?a? ?ts? e??p??ete? t?? a????e? ???? t?? d??t???
  es?te????, µe ???s? d?a???ß?µ???? p??t?p??
  a?af???? ?e?µ???as?a?

23
p??t?pa a?af???? t?? ???? ??????s?µa ?? p??? ta
d?e??? p??t?pa

• p???µet?? µe 10 a?s??t??e? a?t?stas?? ap? Pt µe
  pe????? ?e?t?????a? ap? -80?C ??? 250?C (Agilent
  34972A)

• a?a??t???? ????? p??te de?ad???? ??f???
  (KERN abt 220-5dm)

accredited
24
d?ad??as?e? es?te????? d?a???ß?s??

• t? e??ast???? ??a t? d?e????e?a t?? d?a???ß?se??
• a??????e? d?e??? p??t?pa d?a???ß?s?? (p?. DKD-R
  5-7 ??a d?a???ß?se?? pe??ßa????t???? ?a??µ??, ISO
  8655-2, ISO 8655-6 ?a? PTB-Mitteilungen 112 ??a
  ????µet???? e??p??sµ?, LAB GTA 08 ??a ta
  ?e?µ?µet?a)
• d?a??te? ?a? efa?µ??e? t?p?p???µ??? d?ad??as?a
  ??a t? d?a???ß?s? t?? e??p??sµ??
• d?a??te? d?ad??as?a ?p?????sµ?? t?? aßeßa??t?ta?,
  s??e?t?µ??ta? ??e? t?? ep?µ????? s???st?se?

ta ap?te??sµata t?? d?ad??as??? ?a? ? a???????s?
t??? te?µ???????ta? se ??t?pa t?? s?st?µat??
p???t?ta? (p?.
p?st?p???t??? d?a???ß?s??, ??t?pa a???????s??
p?st?p???t????), ?p?? apa?te?ta? ap? t? p??t?p?
ISO 17025
?? es?te????? d?a???ß?se?? e?t?µ??ta? ap? t? ?S??
?at? t?? a???????s? t?? e??ast?????
25
pa??de??µa es?te????? d?a???ß?s?? ?a??µ??
e?e???µe??? ?e?µ???as?a?
26
p??d?a??af?? ?a??µ?? p?? ?p??e??ta? se d?a???ß?s?

• p??pe? ?a ?p?????? a?s??t??e? ?a? d?at??e??
  e?????? ?e?µ???as?a? µe e?de??e?? ?? s?stat???
  st???e?? t?? ?a??µ??
• p??pe? ?a d?asfa???eta? ? ?s?st??µ?s? t?? p?es??
  st?? ?f???µ? ???? µe t?? atµ?sfa????? p?es?
• p??pe? ?a d?a??te? e?e??? ???µa?s? ?/?a? ????

27
p??d?a??af?? ?a??µ?? p?? ?p??e??ta? se d?a???ß?s?
(s????e?a)

• ?. T??aµ?? µe e?e??? ?????f???a a??a st?? ?f???µ?
  ????
• ?. T??aµ?? ????? e?e??? ?????f???a a??a st??
  ?f???µ? ????
• 
  DKD-R5-7

• µ???st? e???? d?a???ß?s?? ?e?µ???as?a? -90 C
  ??? 500 C
• ?f???µ?? ????? lt 2000 l, t??????st?? 9 ??????
  s?µe?a µ?t??s??
• (8 ????a?? s?µe?a 1 s?µe?? st? ???t?? ???t??
  ??ß??)
• 3. ?f???µ?? ????? gt 2000 l, ?????? s?µe?a
  µ?t??s?? se ??ß??? p???µa
• µe p?e??? 1 m

• µ???st? e???? d?a???ß?s?? ?e?µ???as?a? -90 C
  ??? 350 C
• µ???st?? ?f???µ?? ????? d?a???ß?s?? 2000 l,
  t??????st?? 9 ?????? s?µe?a µ?t??s??
• ?? µet??se?? a??????? t??????st?? 30? µet? t??
  sta?e??p???s? t??
• ?e?µ???as?a?

28
d?ad??as?a d?a???ß?s?? ?a??µ?? ?e?µ???as?a?

• t?p???t?s? 10 a?s??t???? ?e?µ???as?a? st?
  es?te???? t?? ?a??µ?? ?ts? ?ste ?a d?µ?????e?ta?
  p???µa t? ?p??? ?a ?a??pte? st? µ???st? t?? ????
• ?ta? ? ???aµ?? sta?e??p????e? st?? ?e?µ???as?a
  d?a???ß?s?? ???eta? ?ata??af? t?? ?e?µ???as???
  ??a d??st?µa µ?s?? ??a? a?? ??a ?ept?
• ap? t? stat?st??? epe?e??as?a t?? ded?µ????
  p????pt??? ? ??????? ast??e?a ?a? ? ??????
  a??µ??????e?a t?? ?a??µ??, ?a?????eta? ? d?????s?
  ??de???? ? t?? ap????s?? µeta?? t?? ?a??µ?? ?a?
  t?? p??t?p?? a?af???? ?a? ?p??????eta? ?
  aßeßa??t?ta t?? ???????
• s?µp?????eta? t? p?st?p???t??? d?a???ß?s?? ?a?
  ???eta? a???????s? a?t?? ?aµß????ta? ?p??? t??
  apa?t?se?? t?? e??st?te µe??d?? d???µ??
  (p.? 201 C p??sd????sµ?? BOD)
• t? ???a?? f??e? et???ta µe a?a??af?µe?? t??
  ?µe??µ???a d?a???ß?s??, t?? ?µe??µ???a ep?µe???
  d?a???ß?s?? ?a??? ?a? t? d?????s? st?? ??de???
  t?? ?a??µ?? ?p?? apa?te?ta?

29
ep????? s?µe??? e??????

• 9 s?µe?a (8 ????a?? s?µe?a 1 s?µe?? st? ???t??
  ???t?? ??ß??)
• µ???st?? ?f???µ?? ?????
• µ???st? ap?stas? ap? ta t????µata 5 cm
• 10? a?s??t???? ??a ep?d?as? a?t???ß???a?

30
pa?????te? p?? s??e?sf????? st?? aßeßa??t?ta t??
µ?t??s?? (1)

• ? ?????? a??µ??????e?a ?e?µ???as?a? (d? inhom
  )t?? ?a??µ?? ????eta? ?? ? µ???st? ap????s? t??
  ?e?µ???as?a? e??? ????a??? ? p?e?????? s?µe???
  µ?t??s?? ap? t? s?µe?? a?af???? µ?t??s??
• ? ??????? ast??e?a (d? instab) t?? ?a??µ?? ?
  ?p??a ?a?????eta? µe t?? ?ata??af? t??
  ?e?µ???as??? ??a d??st?µa 30 min a?? 1 min
  ????eta? ?? ? µ???st? ap????s? t?? ?e?µ???as?a?
  e??? s?µe??? µ?t??s?? ap? t?? µ?s? t?µ? t??
  ?e?µ???as??? st? d??st?µa t?? µ?s?? ??a?

31
pa?????te? p?? s??e?sf????? st?? aßeßa??t?ta t??
µ?t??s?? (2)

• G?a t?? ep?d?as? t?? a?t???ß???a? (d?radiation)
  t?? ?a??µ?? t? e??ast???? ???s?µ?p??e? ??a
  ?e?µ?µet?? µe ????? s??te?est? ap????f?s?? ?a?
  e?p?µp??( 10?? a?s??t??a? µe µa??? ep???????), t?
  ?p??? t?p??ete?ta? p??s??? t?? a?s??t??a a?af????
  st? ???t?? t?? ?a??µ??. ? ap????s? t?? d??
  ?e?µ?µ?t??? ?e??e?ta? ?t? ?fe??eta? st?? ep?d?as?
  t?? a?t???ß???a?
• ? d?a???t??? ??a??t?ta t?? ?a??µ?? (d?res)
  ????eta? ?? t? te?e?ta?? de?ad??? ??f?? t??
  ??de???? t?? ?a??µ??
• ? aßeßa??t?ta µ?t??s?? t?? p??t?p?? ?e?µ?µ?t???
  a?af???? (d?std) ap? t? p?st?p???t??? d?a???ß?s??

32
?p?????sµ?? s???????? aßeßa??t?ta? ?a??µ??
33
p?st?p???t??? d?a???ß?s?? ?a??µ??

• ?? p?st?p???t??? d?a???ß?s?? f??e?
  t??????st?? t?? a??????e? p????f???e?
• t?? t?t?? p?st?p???t??? d?a???ß?s??
• ?µe??µ???a ?a? t?p? d?a???ß?s??
• saf? p??sd????sµ? ta?t?t?ta? a?t??e?µ???? p??
  d?a???ß????e
• p??sd????sµ? ta?t?t?ta? µe??d?? ?a? e??p??sµ??
• pe??ßa????t???? s?????e?
• ?ept?µe?? pe????af? t?? d?ad??as?a? p??
  a??????????e
• ap?te??sµata d?a???ß?s??
• aßeßa??t?ta µ?t??s??

34
a???????s? p?st?p???t????

• ? a???????s? t?? p?st?p???t???? ß?se? t??
  s?st?µat?? p???t?ta? t?? e??ast????? ???eta? ap?
  t?? ?pe????? p???t?ta? se s??e??as?a µe t??
  te????? ?pe????? ?a? µe t? ß???e?a e???
  ????sµ???? ?p?? t?p??et???ta? ta e???µata t??
  d?ad??as?a? ?a? s????????ta? µe t?? a????? ?a?
  t?? apa?t?se?? p?? ?p?????? st?? µe??d???

35
e????e?e? a???????s?? p?st?p???t???? d?a???ß?s??
?a??µ?? e?e???µe??? ?e?µ???as?a?
e??a? ? aßeßa??t?ta p?? a?a???feta? st?
p?st?p???t??? µ????te?? ap? t??
µ???st? ep?t?ept? ap????s?
ß??s???ta? ?? ?e?µ???as?a??? d?a??µ??se?? ????
t?? s?µe??? e?t?? ?????
???
???
?p?????sµ?? d?????s?? set point ?a? ?e???t????
?p?????sµ?? d?a??µa?s?? ?e?µ???as?a?
???
? ???aµ?? µp??e? ?a ???s?µ?p????e? ?aµß????ta?
?p??? t? d?????s? t?? set point ?a? t????
pe?????sµ??? st? ???s?
???
? ???aµ?? µp??e? ?a ???s?µ?p????e? ?aµß????ta?
?p??? t???? pe?????sµ??? st? ???s?
? ??????? ast??e?a ?e?µ???as?a? e??a? µ????te??
ap? t? µ???st? ep?t?ept? ap????s?
ep?s?e?? ?a??µ?? ?a? e? ???? d?a???ß?s?
???
???
ap?????? t?? ??s?? p?? ?a?????e? t? ??????
a??µ??????e?a ?a? e? ???? ?p?????sµ?? t??
aßeßa??t?ta? d?a???ß?s??
e??a? ? aßeßa??t?ta µ????te?? ap? t? µ???st?
ep?t?ept? ap????s?
???
36
St???? µa? ? s??e?? ße?t??s?

• ??ta?? ?e?te??? µe??d??????? st?? d?ad??as?e? µa?
• ?????t? e??ast???a?? ?????? t?? a??a??µe???
  a?a???? se ??µata d?µ?s?a? ??e?a?

??asf???s? p???t?ta? ap?te?esµ?t??
37
ß?ß?????af?a

1. ISO 170252005 Ge????? apa?t?se?? ??a t??
   ??a??t?ta t?? e??ast????? d???µ?? ?a?
   d?a???ß?se??
2. EA 4/102002 Accreditation for microbiological
   laboratories
3. ?S?? ??1-?????2007 S?st?µata µ?t??s?? ?a?
   d?a???ß?s??
4. DKD-R 5-72009 Calibration of Climatic Chambers
5. UKAS LAB 112012 Traceability of Temperature
   Measurement