Title: QA/QC FOR ENVIRONMENTAL MEASUREMENT
1QA/QC FOR ENVIRONMENTAL MEASUREMENT
- Unit 4 Module 13, Lecture 3
2Objectives
- Introduce Quality Assurance Project Plans (QAPPs)
- What is a QAPP?
- Why is it necessary?
- Explain the processes to take when developing a
QAPP - Eight steps
- Discuss in detail elements to consider and
include when developing a QAPP - 24 elements
3Quality Assurance Project Plans (QAPP)
- QAPP guides
- the selection of parameters and procedures
- data management and analysis
- steps taken to determine the validity of specific
sampling or analysis procedures
- The QAPP outlines the QC measures to be taken for
the project. - The QAPP is a project-specific QA document.
4QA for environmental measurement
- Why do we need quality assurance for
environmental measurement? - understand data reliability
- quantify areas of analytical uncertainty
- standardize measurement to allow for repeatable
and comparable data across time and place
QA ensures that data will meet defined standards
of quality with a standard level of confidence
5Elements of a QAPP
- QAPP can be broken out into four areas of the
project - Project management
- Measurement and data acquisition
- Assessment and oversight
- Data validation and usability
6Establishing a QAPP
- What do you first do when establishing a QAPP?
- Consider the purpose of the investigation
- Compliance vs. background data, etc.
- Consider who is funding the investigation and who
will use that data - What rigor is desired / monetarily feasible?
- Will liability be an issue?
Summarize the purpose of your project
7Steps taken to develop a QAPP
- Establish a QAPP team
- Determine project goals objectives
- Collect background
- Determine project data requirements
- Develop implementation plans
- Develop SOPs
- Draft the QAPP, solicit feed back, revise and
submit for approval - Begin the project, evaluate and redefine QAPP
8Steps taken to develop a QAPP
- Establish a QAPP team
- Include project stakeholders
- technical expertise in varying areas of the
project - Approval required by the governing agency?
- review agency website
- guidance document(s)
9Steps taken to develop a QAPP
- Determine goals and objectives
- Why is the program being conducted?
- Compliance
- Gathering background
- How will the information gathered be used and who
will use it? - Identify all potential data users
- Will collected data be considered useable, and to
what extent? - Comparable to previous work
- Acceptable level of accuracy
10Steps taken to develop a QAPP
- Collect background and redefine the project
- History of the site
- Sources of concern
- Previous investigations / collected data
- Site location and layout
- Geography and weather
- Watershed survey
- Access safety concerns
- Hazards
- Natural
- Manmade
11Steps taken to develop a QAPP
- Design project sampling, analytical and data
requirements - What parameters will be monitored?
- How accurate will the data need to be?
- What are the Data Quality Objectives (DQOs)?
- Where will samples be collected and how will
sites be chosen? - When will sampling be implemented?
- What protocols will be used?
- How will data credibility be assured?
12Steps taken to develop a QAPP
- Develop implementation plans
- Who will carry out the project tasks?
- Sampling, data management / evaluation, etc.
- When will the tasks be conducted?
- How much time will be allotted for each?
- Final report to be generated?
13Steps taken to develop a QAPP
- Adopt or develop project-specific Standard
Operating Procedures (SOPs) - Use industry existing SOPs when possible
- Consistency and usability of data
- Reference and cite sources
- Provide to the field crew as a manual of
instructions
14Steps taken to develop a QAPP
- Draft the QAPP, solicit feedback, and submit for
final approval - Use formats provided by the governing agency or
client - Generate a draft document and solicit feed back
from agency or client prior to implementation - Avoids costly mistakes
- Provide a final revised document to appropriate
project stakeholders
15Steps taken to develop a QAPP
- Begin the monitoring program
- Implement the project as tasked and scheduled
- Evaluate and redefine the QAPP
- What does/ does not work?
- Revise as needed
16Outline of elements in a QAPP
- The four parts and the elements listed under each
- Project Management (elements 1-9)
- Measurement and Data Acquisition (elements 10
19) - Assessment and Oversight (elements 20-21)
- Data Validation and Usability (elements 22-24)
17Outline of elements in a QAPP
- Project Management (elements 1-9)
- Title and Approval Page
- Table of Contents
- Distribution List
- Project / Task Organization
- Problem Identification and Background
- Project/Task Description
- Data Quality Objectives for Measurement Data
- Training Requirement/ Certification
- Documentation and records
18Outline of elements in a QAPP - Management
- Title and Approval Page (element 1)
- Principal investigator(s)
- Project QA officer(s)
- Client Representative
- Table of Contents (element 2)
- Distribution List (element 3)
19Outline of elements in a QAPP Management
- Project / Task Organization
- (element 4)
- Who will participate?
- What are their roles?
20Outline of elements in a QAPP - Management
- Problem Identification and Background (element 5)
- Investigation history
- Site specific
- Regional investigations
- Site background
- Setting rural / industrial
- Geography and climate
- Regional geology, surface water and groundwater
21Outline of elements in a QAPP - Management
- Project/Task Description (element 6)
- What are the tasks?
- When will they take place?
22Outline of elements in a QAPP- Management
- Data Quality Objectives (DQOs) for Measurement
Data (element 7) - Minimum detection limits
- Requirements for detection range
- Training Requirement/
- Certification (element 8)
- Technical proficiency
- Health and safety
23Outline of elements in a QAPP - Management
- Documentation and records (element 9)
- Field and Laboratory
- Raw data
- QC checks
- Field data sheets
- Lab forms
- Voucher collections
24Outline of elements in a QAPP
- Measurement and Data Acquisition (Sections 10
through 19) - Sampling Process Design
- Sampling methods requirement
- Sampling handling and custody requirements
- Analytical Methods requirement
- Quality Control Requirements
25Outline of elements in a QAPP
- Measurement and Data Acquisition (continued
Sections 10 through 19) - Instrument / Equipment Testing, Inspection, and
maintenance requirements - Instrument Calibration and Frequency
- Inspection/Acceptance Requirements for Supplies
- Data Acquisition Requirements
- Data Management
26Outline of elements in a QAPP Data
- Sampling Process Design (element 10)
- Type
- Location
- Frequency of samples
- Sampling period
27Outline of elements in a QAPP - Data
- Sampling methods requirement (element 11)
- Parameter
- Methods
- Collection
- Equipment
- Preservation
- Refer to SOPs
28Outline of elements in a QAPP - Data
29Outline of elements in a QAPP -Data
- Sampling handling and custody requirements
(element 12)
30Outline of elements in a QAPP - Data
- Analytical Methods requirement (element 13)
- Standardized
- ASTM
- EPA
- State modified
- Field adapted
- Instrument manufacture specified
31Outline of elements in a QAPP - Data
- Quality Control Requirements (element 14)
- field blank
- equipment or rinsate blank
- duplicate/replicate samples
- spiked samples
- split and blind samples
32Outline of elements in a QAPP - Data
- Instrument / equipment testing, inspection, and
maintenance requirements (element 15) - Include schedule
- Instrument calibration frequency (element 16)
- Standards
- Frequency
- Inspection/acceptance requirements for supplies
(element 17)
33Outline of elements in a QAPP - Data
- Data Acquisition Requirements (element 18)
- Background information and data
- Previous investigations
- Topographic, geologic, hydrologic or
hydrogeologic - Other monitoring programs, groups or agencies
- Outside source data
- Specific weather conditions barometric pressure
- Note any limitations/questions on data quality
34Outline of elements in a QAPP - Data
- Data Management (element 19)
- Summarize all steps used in data collection and
evaluation - Completeness and accuracy
- Evaluation (computer hardware and softer)
- Minimization of errors
- Data entry
- Backup
- Storage
35Outline of elements in a QAPP
- Assessment and Oversight (elements 20-21)
- Assessment and Response Actions
- Reports
- Data Validation and Usability (elements 22-24)
- Data Review, Validation, and Verification
Requirements - Validation and verification of methods
- Reconciliation with Data Quality Objectives
36Outline of elements in a QAPP
- Assessment and Response Actions (element 20)
- Evaluation of players - audits
- external programs
- field staff
- data management
- Correction of problems
- Reports (element 21)
- Frequency, content, distribution
37Outline of elements in a QAPP
- Data Review, Validation, and Verification
Requirements (element 22) - Indicate what will be done and by whom
- Validation and verification of methods (element
23) - Indicate procedures to be used
- Reconciliation with Data Quality Objectives
(element 24) - Determining if project objectives have been met
38References
- Some References on Environmental Quality
Assurance Plans - EPA 240/B-01-002 . EPA Requirements for Quality
Management Plans (QA/R-2). March 2001.
(http//www.epa.gov/quality1/qa_docs.html) - EPA 240/B-01-003. EPA Requirements for QA
Project Plans (QA/R-5). March 2001. - EPA 430/9-86-004. Quality Assurance/Quality
Control (QA/QC) for 301(h) Monitoring Programs
Guidance on Field and Laboratory Methods. March
1987. (NTIS / PB87-221164) - EPA 440/4-91-002 . Volunteer Lake Monitoring.
December 1991. (http//www.epa.gov/OWOW/monitori
ng/volunteer/lake/index.html)
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